Overview
ISO 1064:1974 is an international standard published by the International Organization for Standardization (ISO) that specifies a laboratory method for determining the apparent density of surface active agents presented in paste form. This standard focuses on measuring the apparent density of pastes, ointments, and similar viscous products during the filling process. Accurate determination of apparent density is critical for quality control and formulation consistency in industries dealing with surfactants and paste-like materials.
Key Topics
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Apparent Density Measurement
The standard defines a laboratory procedure to measure the apparent density of pasty surface active agents at a controlled temperature of 20°C. It involves filling a known volume container under controlled pressure and conditions.
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Test Apparatus
The method requires specific equipment, including:
- A stainless steel tube with defined dimensions
- A stainless steel piston with a precise weight and diameter
- A rigid cylindrical container for sample filling of fixed volume (50 ml), diameter, and height
- A height-adjustable support with an articulated device for controlled filling speed
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Test Procedure
The procedure involves placing the sample in the steel tube, inserting the piston with additional weights to ensure a steady flow, and slowly lowering the container to be filled from below. The air trapped is released via an annular space between the tube and container. After filling, excess sample is trimmed to create a level surface.
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Calculations and Results
Apparent density (in grams per milliliter) is calculated by weighing the filled container, subtracting container mass, and dividing by container volume. The average of five determinations is recommended for accuracy. Repeatability requires results between duplicate tests by the same operator not to differ by more than 0.1 g/ml.
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Documentation
Complete test reports must include paste identification, concentration, measurement temperature, container volume, filling time, sample weight, and any deviations or unusual observations.
Applications
ISO 1064:1974 is especially relevant for industries and laboratories involved in:
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Surfactant Paste Manufacturing
Ensuring consistent batch density for quality and performance characteristics.
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Pharmaceuticals and Cosmetics
Formulating ointments, creams, and gels where accurate density impacts dosage and texture control.
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Chemical Quality Control
Standardized density data supports product specification and regulatory compliance.
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Research and Development
Facilitating comparative studies of surface active agents in paste form to optimize formulations.
Related Standards
While ISO 1064:1974 specifically targets apparent density measurement of paste form surface active agents, it interfaces with related standards including:
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ISO Methods for Surfactant Sample Preparation
Guidelines for preparing representative test samples of surface active agents in various states.
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ISO Standards on Density Measurement
Broader density determination methods for liquids, solids, and powders complementing paste measurements.
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Industry-specific Standards
Pharmaceutical and cosmetic standards that reference density as a critical quality parameter.
Keywords: ISO 1064, apparent density, surface active agents, surfactant pastes, density measurement, laboratory method, paste filling, quality control, pharmaceutical ointments, cosmetic creams, standard test procedure.