ISO 685:1975 PDF

The method consists in decomposition of the soap by a known volume of standard volumetric mineral acid solution, extraction and separation of the liberated fatty matter with light petroleum and determination of a total alkali content by titration of the excess of acid contained in the aqueous phase with a standard volumetric sodium hydroxide solution. After evaporation of the light petroleum from the extract, dissolution of the residue in ethanol and neutralization of the fatty acids with a standard volumetric potassium hydroxide solution. Evaporation of the ethanol and weighing of the soap formed to determine the total fatty matter content.